Isotope Labeling Reveals Fast Atomic and Molecular Exchange in Mechanochemical Milling Reactions

S. Lukin, M. Tireli, T. Stolar, D. Barišić, M. V. Blanco, M. di Michiel, K. Užarević, I. Halasz - J. Am. Chem Soc. 141 (2019) 1212–1216.

https://doi.org/10.1021/jacs.8b12149

Mechanochemical carbon-carbon bond formation that proceeds via a cocrystals intermediate

S. Lukin, M. Tireli, I. Lončarić, D. Barišić, P. Šket, D. Vrsaljko, M. di Michiel, J. Plavec, K. Užarević, I.  Halasz - Chem Commun. 54 (2018) 13216–13219.

https://doi.org/10.1039/C8CC07853J

Experimental and Theoretical Study of Selectivity in Mechanochemical Cocrystallization of Nicotinamide with Anthranillic and Salicylic Acid

S. Lukin, I. Lončarić, M. Tireli, T. Stolar, M. V. Blanco, P. Lazić, K. Užarević, I. Halasz - Cryst. Growth Des. 18 (2018) 1539–1547.

http://doi.org/10.1021/acs.cgd.7b01512

Enthalpy vs. friction: heat flow modelling of unexpected temperature profiles in mechanochemistry of metal–organic frameworks

K. Užarević, N. Ferdelji, T. Mrla, P. A. Julien, B. Halasz, T. Friščić, I. Halasz - Chem. Sci. 9 (2018) 2525–2532.

https://doi.org/10.1039/C7SC05312F

Tandem in Situ Monitoring for Quantitative Assessment of Mechanochemical Reactions Involving Structurally Unknown Phases

S. Lukin, T. Stolar, M. Tireli, M. V. Blanco, D. Babić, T. Friščić, K. Užarević, I. Halasz - Chem. Eur. J. 23 (2017) 13941–13949.

https://doi.org/10.1002/chem.201702489

In Situ Monitoring and Mechanism of the Mechanochemical Formation of a Microporous MOF–74 Framework

P. A. Julien, K. Užarević, A. D. Katsenic, S. A. J. Kimber, T. Wang, O. K. Farha, Y. Zhang, J. Casaban, L. S. Germann, M. Etter, R. E. Dinnebier, S. L. James, I. Halasz, T. Friščić - J. Am. Chem Soc. 138 (2016) 2929–2932.

https://doi.org/10.1021/jacs.5b13038

In situ X–ray diffraction monitoring of a mechanochemical reaction reveals a unique topology metal–organic framework

A. D. Katsenis, A. Puškarić, V. Štrukil, C. Mottillo, P. A. Julien, K. Užarević, M.–H. Pham, T.–O. Do, S. A. J. Kimber, P. Lazić, O. Magdysyuk, R. E. Dinnebier, I. Halasz, T. Friščić - Nat. Commun. 6 (2015) 6662.

https://www.nature.com/articles/ncomms7662

Laboratory Real-Time and In Situ Monitoring of Mechanochemical Milling Reactions by Raman Spectroscopy

D. Gracin, V. Štrukil, T. Friščić, I. Halasz, K. Užarević - Angew. Chem. Int. Ed. 53 (2014) 6193–6197.

https://doi.org/10.1002/anie.201402334

Real-time and in situ monitoring of mechanochemical milling reactions

T. Friščić, I. Halasz, P. J. Beldon, A. M. Belenguer, F. Adams,S. A. J. Kimber, V. Honkimäki, R. Dinnebier - Nature Chem. 5 (2013) 66–73.

https://doi.org/10.1038/nchem.1505

Journal articles

Scientific and review papers

• Vugrin, L., Halasz, I. & Geneste, H. (2023) Characterization and isolation of an 18-crown-6 complex of potassium hydroxide prepared by milling: application to mechanochemical organic synthesis. New journal of chemistry, 47, 7466-7469 doi:10.1039/D3NJ00364G.

  doi

• Vugrin, L., Carta, M., Delogu, F. & Halasz, I. (2023) Extending the Hammett correlation to mechanochemical reactions. Chemical communications, 59 (12), 1629-1632 doi:10.1039/d2cc06487a.

  doi

• Angerhofer, A., Auvray, T., Balema, V., Baláž, M., Batteas, J., Blair, R., Boldyreva, E., Bolm, C., Borchardt, L., Borchers, T., Braunschweig, A., Browne, D., Carpick, R., Ciaccia, M., Craig, S., Emmerling, F., Ferguson, M., Fiore, C., Friščić, T., Grätz, S., Halasz, I., Hamzehpoor, E., Ito, H., James, S., Kim, J., Lamaty, F., Lampronti, G., Laurencin, D., Leitch, J., Lu, E., Lukin, S., Mack, J., Maini, L., Martini, A., Mazzeo, P., Michalchuk, A., Mittelette, S., Mohamed, S., Moores, A., Mortera-Carbonell, A., Nagapudi, K., Niidu, A., Puccetti, F., Stahorský, M. & Vugrin, L. (2023) Kinetics and basic understanding: general discussion. FARADAY DISCUSSIONS, 241, 306-340 doi:10.1039/d2fd90082c.

  doi

• Vugrin, L., Carta, M., Lukin, S., Meštrović, E., Delogu, F. & Halasz, I. (2023) Mechanochemical reaction kinetics scales linearly with impact energy. FARADAY DISCUSSIONS, 241, 217-229 doi:10.1039/D2FD00083K.

  doi

• Kralj, M., Krivačić, S., Ivanišević, I., Zubak, M., Supina, A., Marciuš, M., Halasz, I. & Kassal, P. (2022) Conductive inks based on melamine intercalated graphene nanosheets for inkjet printed flexible electronics. Nanomaterials, 12 (17), 2936, 15 doi:10.3390/nano12172936.

  doiwww.mdpi.comdx.doi.org

• Ardila‐Fierro, K., Vugrin, L., Halasz, I., Palčić, A. & Hernández, J. (2022) Mechanochemical Bromination of Naphthalene Catalyzed by Zeolites: From Small Scale to Continuous Synthesis. Chemistry methods, 2 (12), e202200035, 6 doi:10.1002/cmtd.202200035.

  doichemistry-europe.onlinelibrary.wiley.comdoi.orgfulir.irb.hr

• Barišić, D., Pajić, M., Halasz, I., Babić, D. & Ćurić, M. (2022) Mechanochemical halogenation of unsymmetrically substituted azobenzenes. Beilstein journal of organic chemistry, 18, 680-687 doi:10.3762/bjoc.18.69.

  doiwww.beilstein-journals.orgdoi.orgfulir.irb.hr

• Puccetti, F., Lukin, S., Užarević, K., Colacino, E., Halasz, I., Bolm, C. & Hernández, J. (2022) Mechanistic Insights on the Mechanosynthesis of Phenytoin, a WHO Essential Medicine. Chemistry : a European journal, 28 (13), e202104409, 5 doi:10.1002/chem.202104409.

  doidoi.orgchemistry-europe.onlinelibrary.wiley.comfulir.irb.hr

• Leszczyński, M., Kornacki, D., Terlecki, M., Justyniak, I., Miletić, G., Halasz, I., Bernatowicz, P., Szejko, V. & Lewiński, J. (2022) Mechanochemical vs Wet Approach for Directing CO2 Capture toward Various Carbonate and Bicarbonate Networks. ACS Sustainable Chemistry & Engineering, 10 (14), 4374-4378 doi:10.1021/acssuschemeng.1c08402.

  doi

• Lukin, S., Germann, L., Friščić, T. & Halasz, I. (2022) Toward Mechanistic Understanding of Mechanochemical Reactions Using Real-Time In Situ Monitoring. Accounts of chemical research, 55 (9), 1262-1277 doi:10.1021/acs.accounts.2c00062.

  doi

• Barišić, D., Halasz, I., Bjelopetrović, A., Babić, D. & Ćurić, M. (2022) Mechanistic Study of the Mechanochemical PdII-Catalyzed Bromination of Aromatic C–H bonds by Experimental and Computational methods. Organometallics, 41 (11), 1284-1294 doi:10.1021/acs.organomet.1c00698.

  doi

• Szczerba, D., Tan, D., Do, J., Titi, H., Mouhtadi, S., Chaumont, D., de Lucas, M., Geoffroy, N., Meyer, M., Rousselin, Y., Hudspeth, J., Schwanen, V., Spoerk-Erdely, P., Dippel, A., Ivashko, O., Gutowski, O., Glaevecke, P., Bazhenov, V., Arhangelskis, M., Halasz, I., Friščić, T. & Kimber. Simon AJ (2021) Real-Time Observation of “Soft” Magic-Size Clusters during Hydrolysis of the Model Metallodrug Bismuth Disalicylate. Journal of the American Chemical Society, 143, 16332-16336 doi:10.1021/jacs.1c07186.

  doi

• Kralj, M., Lukin, S., Miletić, G. & Halasz, I. (2021) Using desmotropes, cocrystals and salts for manipulating reactivity in mechanochemical organic reactions. Journal of organic chemistry, 86 (20), 14160-14168 doi:10.1021/acs.joc.1c01817.

  doi

• Lukin, S., Užarević, K. & Halasz, I. (2021) Raman spectroscopy for real-time and in situ monitoring of mechanochemical milling reactions. Nature Protocols, 16, 3492-3521 doi:10.1038/s41596-021-00545-x.

  doi

• Catalano, L., Germann, L., Julien, P., Arhangelskis, M., Halasz, I., Užarević, K., Etter, M., Dinnebier, R., Ursini, M., Cametti, M., Martí-Rujas, J., Friščić, T., Metrangolo, P., Resnati, G. & Terraneo, G. (2021) Open versus Interpenetrated: Switchable Supramolecular Trajectories in Mechanosynthesis of a Halogen-Bonded Borromean Network. Chem, 7 (1), 146-154 doi:10.1016/j.chempr.2020.10.022.

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• Milanović, I., Biliškov, N., Užarević, K., Lukin, S., Etter, M. & Halasz, I. (2021) Mechanochemical Synthesis and Thermal Dehydrogenation of Novel Calcium-Containing Bimetallic Amidoboranes. ACS Sustainable Chemistry & Engineering, 9 (5), 2089-2099 doi:10.1021/acssuschemeng.0c06839.

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• Fiore, C., Sović, I., Lukin, S., Halasz, I., Martina, K., Delogu, F., Ricci, P., Porcheddu, A., Shemchuk, O., Braga, D., Pirat, J., Virieux, D. & Colacino, E. (2020) Kabachnik–Fields Reaction by Mechanochemistry: New Horizons from Old Methods. ACS Sustainable Chemistry & Engineering, 8 (51), 18889-18902 doi:10.1021/acssuschemeng.0c05744.

  doi

• Lukin, S., Stolar, T., Lončarić, I., Milanović, I., Biliškov, N., di Michiel, M., Friščić, T. & Halasz, I. (2020) Mechanochemical Metathesis between AgNO3 and NaX (X = Cl, Br, I) and Ag2XNO3 Double-Salt Formation. Inorganic chemistry, 59 (17), 12200-12208 doi:10.1021/acs.inorgchem.0c01196.

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• Sović, I., Lukin, S., Meštrović, E., Halasz, I., Porcheddu, A., Delogu, F., Ricci, P., Caron, F., Perilli, T., Dogan, A. & Colacino, E. (2020) Mechanochemical Preparation of Active Pharmaceutical Ingredients Monitored by In Situ Raman Spectroscopy. ACS Omega, 5 (44), 28663-28672 doi:10.1021/acsomega.0c03756.

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• Bjelopetrović, A., Barišić, D., Duvnjak, Z., Džajić, I., Juribašić Kulcsar, M., Halasz, I., Martinez, M., Budimir, A., Babić, D. & Ćurić, M. (2020) A Detailed Kinetico-Mechanistic Investigation on the Palladium C–H Bond Activation in Azobenzenes and Their Monopalladated Derivatives. Inorganic chemistry, 59 (23), 17123-17133 doi:10.1021/acs.inorgchem.0c02418.

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• Stolar, T., Lukin, S., Etter, M., Rajić Linarić, M., Užarević, K., Meštrović, E. & Halasz, I. (2020) DNA-specific selectivity in pairing of model nucleobases in the solid state. Chemical communications, 56, 13524-13527 doi:10.1039/d0cc03491f.

  doi

• Kralj, M., Supina, A., Sović, I., Čapeta, D. & Halasz, I. (2020) Mechanochemical oxidation of graphite for graphene-hydrogel applications: pitfalls and benefits. Materialia, 14, 100908, 9 doi:10.1016/j.mtla.2020.100908.

  doi

• Muratović, S., Karadeniz, B., Stolar, T., Lukin, S., Halasz, I., Herak, M., Mali, G., Krupskaya, Y., Kataev, V., Žilić, D. & Užarević, K. (2020) Impact of dehydration and mechanical amorphization on the magnetic properties of Ni(ii)-MOF-74. Journal of Materials Chemistry C, 8, 7132-7142 doi:10.1039/D0TC00844C.

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• Ardila-Fierro, K., Lukin, S., Etter, M., Užarević, K., Halasz, I., Bolm, C. & Hernández, J. (2020) Direct visualization of a mechanochemically induced molecular rearrangement. Angewandte Chemie. International edition, 59 (32), 13458-13462 doi:10.1002/anie.201914921.

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• Vogt, C., Grätz, S., Lukin, S., Halasz, I., Etter, M., Evans, J. & Borchardt, L. (2019) Direct Mechanocatalysis: Palladium as Milling Media and Catalyst in the Mechanochemical Suzuki Polymerization. Angewandte Chemie. International edition, 58 (52), 18942-18947 doi:10.1002/anie.201911356.

  doidoi.orgonlinelibrary.wiley.com

• Bjelopetrović, A., Robić, M., Halasz, I., Babić, D., Juribašić Kulcsar, M. & Ćurić, M. (2019) Facile Mechanochemical Anion Substitution in Cyclopalladated Azo-benzenes. Organometallics, 38 (22), 4479-4484 doi:10.1021/acs.organomet.9b00626.

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• Stolar, T., Lukin, S., Tireli, M., Sović, I., Karadeniz, B., Kereković, I., Matijašić, G., Gretić, M., Katančić, Z., Dejanović, I., Michiel, M., Halasz, I. & Užarević, K. (2019) Control of pharmaceutical cocrystal polymorphism on various scales by mechanochemistry: transfer from the laboratory batch to the large-scale extrusion processing. ACS Sustainable Chemistry & Engineering, 7 (7), 7102-7110 doi:10.1021/acssuschemeng.9b00043.

  doi

• Lukin, S., Tireli, M., Stolar, T., Barišić, D., Blanco, M., di Michiel, M., Užarević, K. & Halasz, I. (2019) Isotope Labeling Reveals Fast Atomic and Molecular Exchange in Mechanochemical Milling Reactions. Journal of the American Chemical Society, 141 (3), 1212-1216 doi:10.1021/jacs.8b12149.

  doi

• Colacino, E., Porcheddu, A., Halasz, I., Charnay, C., Delogu, F., Guerra, R. & Fullenwarth, J. (2018) Mechanochemistry for “no solvent, no base” preparation of hydantoin-based active pharmaceutical ingredients: nitrofurantoin and dantrolene. Green chemistry, 20 (13), 2973-2977 doi:10.1039/c8gc01345d.

  doi

• Lukin, S., Tireli, M., Lončarić, I., Barišić, D., Šket, P., Vrsaljko, D., di Michiel, M., Plavec, J., Užarević, K. & Halasz, I. (2018) Mechanochemical carbon-carbon bond formation that proceeds via a cocrystal intermediate. Chemical communications, 54, 13216-13219 doi:10.1039/C8CC07853J.

  doi

• Bjelopetrović, A., Lukin, S., Halasz, I., Užarević, K., Đilović, I., Barišić, D., Budimir, A., Juribašić Kulcsar, M. & Ćurić, M. (2018) Mechanism of Mechanochemical C–H Bond Activation in an Azobenzene Substrate by Pd(II) Catalysts. Chemistry : a European journal, 24 (42), 10672-10682 doi:10.1002/chem.201802403.

  doi

• Fidelli, A., Karadeniz, B., Howarth, A., Huskić, I., Germann, L., Halasz, I., Etter, M., Moon, S., Dinnebier, R., Stilinović, V., Farha, O., Friščić, T. & Užarević, K. (2018) Green and rapid mechanosynthesis of high-porosity NU- and UiO-type metal–organic frameworks. Chemical communications, 54 (51), 6999-7002 doi:10.1039/c8cc03189d.

  doi

• Lukin, S., Lončarić, I., Tireli, M., Stolar, T., Blanco, M., Lazić, P., Užarević, K. & Halasz, I. (2018) Experimental and Theoretical Study of Selectivity in Mechanochemical Cocrystallization of Nicotinamide with Anthranilic and Salicylic Acid. Crystal growth & design, 18 (3), 1539-1547 doi:10.1021/acs.cgd.7b01512.

  doi

• Užarević, K., Ferdelji, N., Mrla, T., Julien, P., Halasz, B., Friščić, T. & Halasz, I. (2018) Enthalpy vs. friction: heat flow modelling of unexpected temperature profiles in mechanochemistry of metal–organic frameworks. Chemical Science, 9, 2525-2532 doi:10.1039/c7sc05312f.

  doipubs.rsc.orgpubs.rsc.orgfulir.irb.hr

• Lukin, S., Stolar Tomislav, Tireli, M., Barišić, D., Di Michiel, M., Užarević, K. & Halasz, I. (2017) Solid-State Supramolecular Assembly of Salicylic Acid and 2-Pyridone, 3-Hydroxypyridine or 4-Pyridone. Croatica chemica acta, 90 (4), 707-710 doi:10.5562/cca3339.

  doi

• Biliškov, N., Borgschulte, A., Užarević, K., Halasz, I., Lukin, S., Milošević, S., Milanović, I. & Grbović Novaković, J. (2017) In-situ and Real-time Monitoring of Mechanochemical Preparation of Li2Mg(NH2BH3)4 and Na2Mg(NH2BH3)4 and their Thermal Dehydrogenation. Chemistry : a European journal, 23, 16274-16282 doi:10.1002/chem.201702665.

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• Tireli, M., Maračić, S., Lukin, S., Juribašić Kulcsar, M., Žilić, D., Cetina, M., Halasz, I., Raić-Malić, S. & Užarević, K. (2017) Solvent-free copper-catalyzed click chemistry for the synthesis of N-heterocyclic hybrids based on quinoline and 1,2,3-triazole. Beilstein journal of organic chemistry, 13, 2352-2363 doi:10.3762/bjoc.13.232.

  doiwww.beilstein-journals.org

• Stolar, T., Batzdorf, L., Lukin, S., Žilić, D., Motillo, C., Friščić, T., Emmerling, F., Halasz, I. & Užarević, K. (2017) In Situ Monitoring of the Mechanosynthesis of the Archetypal Metal–Organic Framework HKUST-1 : Effect of Liquid Additives on the Milling Reactivity. Inorganic chemistry, 56 (11), 6599-6608 doi:10.1021/acs.inorgchem.7b00707.

  doi

• Lukin, S., Stolar, T., Tireli, M., Blanco, M., Babić, D., Friščić, T., Užarević, K. & Halasz, I. (2017) Tandem in situ monitoring for quantitative assessment of mechanochemical reactions involving structurally unknown phases. Chemistry : a European journal, 23, 13941-13949 doi:10.1002/chem.201702489.

  doionlinelibrary.wiley.com

• Juribašić Kulcsar, M., Halasz, I., Budimir, A., Užarević, K., Lukin, S., Monas, A., Emmerling, F., Plavec, J. & Ćurić, M. (2017) Reversible Gas−Solid Ammonia N−H Bond Activation Mediated by an Organopalladium Complex. Inorganic chemistry, 56 (9), 5342-5351 doi:10.1021/acs.inorgchem.7b00422.

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• Konnert, L., Gonnet, L., Halasz, I., Suppo, J., de Figueiredo, R., Campagne, J., Lamaty, F., Martinez, J. & Colacino, E. (2016) Mechanochemical Preparation of 3, 5-Disubstituted Hydantoins from Dipeptides and Unsymmetrical Ureas of Amino Acid Derivatives. Journal of organic chemistry, 81 (20), 9802-9809 doi:10.1021/acs.joc.6b01832.

  doi

• Corpinot, M., Stratford, S., Arhangelskis, M., Anka-Lufford, J., Halasz, I., Judaš, N., Jones, W. & Bučar, D. (2016) On the predictability of supramolecular interactions in molecular cocrystals – the view from the bench. Crystengcomm, 18 (29), 5434-5439 doi:10.1039/c6ce00293e.

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• Monas, A., Užarević, K., Halasz, I., Juribašić Kulcsar, M. & Ćurić, M. (2016) Vapour-induced solid-state C–H bond activation for the clean synthesis of an organopalladium biothiol sensor. Chemical communications, 52 (88), 12960-12963 doi:10.1039/c6cc06062e.

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• Stolar, T., Lukin, S., Požar, J., Rubčić, M., Day, G., Biljan, I., Šišak Jung, D., Horvat, G., Užarević, K., Meštrović, E. & Halasz, I. (2016) Solid-State Chemistry and Polymorphism of the Nucleobase Adenine. Crystal growth & design, 16 (6), 3262-3270 doi:10.1021/acs.cgd.6b00243.

  doi

• Užarević, K., Štrukil, V., Mottillo, C., Julien, P., Puškarić, A., Friščić, T. & Halasz, I. (2016) Exploring the effect of temperature on a mechanochemical reaction by in situ synchrotron powder X-ray diffraction. Crystal growth & design, 16 (4), 2342-2347 doi:10.1021/acs.cgd.6b00137.

  doi

• Julien, P., Užarević, K., Katsenis, A., Kimber, S., Wang, T., Farha, O., Zhang, Y., Casaban, J., Germann, L., Etter, M., Dinnebier, R., James, S., Halasz, I. & Friščić, T. (2016) In situ monitoring and mechanism of the mechanochemical formation of a microporous MOF-74 framework. Journal of the American Chemical Society, 138 (9), 2929-2932 doi:10.1021/jacs.5b13038.

  doi

• Puškarić, A., Halasz, I., Gredičak, M., Palčić, A. & Bronić, J. (2016) Synthesis and structure characterization of zinc and cadmium dipeptide coordination polymers. New journal of chemistry, 40, 4252-4257 doi:10.1039/c5nj03001c.

  doi

• Cindro, N., Antol, I., Mlinarić-Majerski, K., Halasz, I., Wan, P. & Basarić, N. (2015) Reactivity of cations and zwitterions formed in photochemical and acid-catalyzed reactions from m-hydroxycycloalkyl substituted phenol derivatives. Journal of organic chemistry, 80 (24), 12420-12430 doi:10.1021/acs.joc.5b02297.

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• Užarević, K., Halasz, I. & Friščić, T. (2015) Real-Time and In Situ Monitoring of Mechanochemical Reactions : A New Playground for All Chemists. Journal of physical chemistry letters, 6 (20), 4129-4140 doi:10.1021/acs.jpclett.5b01837.

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• Blažek Bregović, V., Halasz, I., Basarić, N. & Mlinarić-Majerski, K. (2015) Anthracene adamantylbisurea receptors: switching of anion binding by photocyclization. Tetrahedron, 71, 9321-9327 doi:10.1016/j.tet.2015.10.013.

  doi

• Katsenis, A., Puškarić, A., Štrukil, V., Mottillo, C., Julien, P., Užarević, K., Pham, M., Do, T., Kimber, S., Lazić, P., Magdysyuk, O., Dinnebier, R., Halasz, I. & Friščić, T. (2015) In situ X-ray diffraction monitoring of a mechanochemical reaction reveals a unique topology metal-organic framework. Nature Communications, 6, 6662-1 doi:10.1038/ncomms7662.

  doi

• Tireli, M., Juribašić Kulcsar, M., Cindro, N., Gracin, D., Biliškov, N., Borovina, M., Ćurić, M., Halasz, I. & Užarević, K. (2015) Mechanochemical reactions studied by in situ Raman spectroscopy : base catalysis in liquid-assisted grinding. Chemical communications, 51 (38), 8058-8061 doi:10.1039/c5cc01915j.

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• Džeba, I., Halasz, I., Lukić-Glavaš, K. & Vančik, H. (2014) Mechanochemically induced anion exchange in minoazobenzene salts. Croatica chemica acta, 87 (4), 407-412 doi:10.5562/cca2485.

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• Cvetešić, N., Palencia, A., Halasz, I., Cusack, S. & Gruić-Sovulj, I. (2014) The physiological target for LeuRS translational quality control is norvaline. EMBO journal, 33 (15), 1639-1653 doi:10.15252/embj.201488199.

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• Rubčić, M., Galić, N., Halasz, I., Jednačak, T., Judaš, N., Plavec, J., Šket, P. & Novak, P. (2014) Multiple solid forms of 1, 5-bis(salicylidene)carbohydrazide : polymorph-modulated thermal reactivity. Crystal growth & design, 14 (6), 2900-2912 doi:10.1021/cg500203k.

  doi

• Gracin, D., Štrukil, V., Friščić, T., Halasz, I. & Užarević, K. (2014) Laboratory real-time and in situ monitoring of mechanochemical milling reactions using Raman spectroscopy. Angewandte Chemie. International edition, 53 (24), 6193-6197 doi:10.1002/anie.201402334.

  doifulir.irb.hr

• Halasz, I., Friščić, T., Kimber, S., Užarević, K., Puškarić, A., Mottillo, C., Julien, P., Štrukil, V., Honkimäki, V. & Dinnebier, R. (2014) Quantitative in situ and real-time monitoring of mechanochemical reactions. Faraday discussions, 170, 203-221 doi:10.1039/C4FD00013G.

  doi

• Juribašić, M., Halasz, I., Babić, D., Cinčić, D., Plavec, J. & Ćurić, M. (2014) Aging and Ball-Milling as Low-Energy and Environmentaly-Friendly Methods for the Synthesis of Pd(II) Photosensitizers. Organometallics, 33 (5), 1227-1234 doi:10.1021/om500008v.

  doi

• Maganjić, A., Šolić, I., Milovac, S., Halasz, I., Biljan, I. & Vančik, H. (2014) Mechanochemically induced cross-dimerizations of nitrosobenzenes. Kinetics and solid-state isotope effects. Journal of physical organic chemistry, 27 (3), 177-182 doi:1002/poc.3256.

  doi

• Palčić, A., Halasz, I. & Bronić, J. (2014) Crystal structure of copper(II) citrate monohydrate solved from a mixture powder X-ray diffraction pattern. Powder diffraction, 29 (1), 28-32 doi:10.1017/S0885715613001267.

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• Bučar, D., Day, G., Halasz, I., Zhang, G., Sander, J., Reid, D., MacGillivray, L., Duer, M. & Jones, W. (2013) The curious case of (caffeine)·(benzoic acid): how heteronuclear seeding allowed the formation of an elusive cocrystal. Chemical Science, 4 (12), 4417-4425 doi:10.1039/C3SC51419F.

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• Halasz, I., Puškarić, A., Kimber, S., Beldon, P., Belenguer, A., Adams, F., Honkimäki, V., Dinnebier, R., Patel, B., Jones, W., Štrukil, V. & Friščić, T. (2013) Real-Time In Situ Powder X-ray Diffraction Monitoring of Mechanochemical Synthesis of Pharmaceutical Cocrystals. Angewandte Chemie. International edition, 52 (44), 11538-11541 doi:10.1002/anie.201305928.

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• Halasz, I., Kimber, S., Beldon, P., Belenguer, A., Adams, Frank, Honkimäki, Veijo, Nightingale, R., Dinnebier, R. & Friščić, T. (2013) In situ and real-time monitoring of mechanochemical milling reactions using synchrotron X-ray diffraction. Nature protocols, 8, 1718-1729 doi:10.1038/nprot.2013.100.

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• Halasz, I., Cindro, N., Dinnebier, R. & Vančik, H. (2013) An Old Story in New Light: X-Ray Powder Diffraction Provides Novel Insights into a Long-Known Organic Solid-State Rearrangement Reaction. Croatica chemica acta, 86 (2), 187-192 doi:10.5562/cca2127.

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• Užarević, K., Halasz, I., Đilović, I., Bregović, N., Rubčić, M., Matković-Čalogović, D. & Tomišić, V. (2013) Dynamic Molecular Recognition in Solid State for Separating Mixtures of Isomeric Dicarboxylic Acids. Angewandte Chemie. International edition, 52 (21), 5504-5508 doi:10.1002/anie.201301032.

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• Stilinović, V., Bučar, D., Halasz, I. & Meštrović, E. (2013) V=O...C interactions in crystal structures of oxovanadium-coordination compounds. New journal of chemistry, 37 (3), 619-623 doi:10.1039/C2NJ40780A.

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• Alešković, M., Basarić, N., Halasz, I., Liang, X., Qinc, W. & Mlinarić-Majerski, K. (2013) Aryl substituted adamantane-dipyrromethanes: Chromogenic and fluorescent anion sensors. Tetrahedron, 69, 1725-1734 doi:10.1016/j.tet.2012.12.026.

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• Friščić, T., Halasz, I., Beldon, P., Belenguer, A., Adams, F., Kimber, S., Honkimaeki, V. & Dinnebier, R. (2013) Real-time and in situ monitoring of mechanochemical milling reactions. Nature Chemistry, 5, 66-73 doi:10.1038/NCHEM.1505.

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• Cindro, N., Halasz, I., Mlinarić-Majerski, K. & Basarić, N. (2013) Photoinduced H-abstraction in homo- and protoadamantylphthalimide derivatives in solution and in organized and constrained media. European journal of organic chemistry, (5), 929-938 doi:10.1002/ejoc.201201332.

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• Halasz, I., Dinnebier, R., Chiodo, T. & Saxell, H. (2012) Structures of four polymorphs of the pesticide dithianon solved from X-ray powder diffraction data. Acta crystallographica. Section B, Structural science, 68 (6), 661-666 doi:10.1107/S0108768112036191.

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• Štrukil, V., Bartolec, B., Portada, T., Đilović, I., Halasz, I. & Margetić, D. (2012) One-pot mechanosynthesis of aromatic amides and dipeptides from carboxylic acids and amines. Chemical communications, 48 (99), 12100-12102 doi:10.1039/C2CC36613D.

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• Štrukil, V., Igrc, M., Fábián, L., Eckert-Maksić, M., Childs, S., Reid, D., Duer, M., Halasz, I., Mottilloe, C. & Friščić, T. (2012) A model for a solvent-free synthetic organic research laboratory: click-mechanosynthesis and structural characterization of thioureas without bulk solvents. Green chemistry, 14 (9), 2462-2473 doi:10.1039/C2GC35799B.

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• Huskić, I., Halasz, I., Friščić, T. & Vančik, H. (2012) Mechanosynthesis of nitrosobenzenes: a proof-of-principle study in combining solvent-free synthesis with solvent-free separations. Green chemistry, 14, 1597-1600 doi:10.1039/c2gc35410a.

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• Rubčić, M., Užarević, K., Halasz, I., Bregović, N., Mališ, M., Đilović, I., Kokan, Z., Stein, R., Dinnebier, R. & Tomišić, V. (2012) Desmotropy, Polymorphism, and Solid-State Proton Transfer : Four Solid Forms of an Aromatic o-Hydroxy Schiff Base. Chemistry : a European journal, 18 (18), 5620-5631 doi:10.1002/chem.201103508.

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• Cindrić, M., Uzelac, M., Cinčić, D., Halasz, I., Pavlović, G., Hrenar, T., Ćurić, M. & Kovačević, D. (2012) Three routes to nickel(II) salicylaldehyde 4-phenyl and 4-methylthiosemicarbazonato complexes: mechanochemical, electrochemical and conventional approach. Crystengcomm, 14, 3039-3045 doi:10.1039/c2ce06611d.

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• Friščić, T., Halasz, I., Štrukil, V., Eckert-Maksić, M. & Dinnebier, R. (2012) Clean and efficient synthesis using mechanochemistry : coordination polymers, open metal-organic frameworks and metallodrugs. Croatica chemica acta, 85 (3), 367-378 doi:10.5562/cca2014.

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• Biljan, I., Halasz, I., Milovac, S. & Vančik, H. (2012) In Search for Universal Models. Dimerization of Nitrosobenzenes and Investigation of Some Basic Chemical Concepts. Kemija u industriji : časopis kemičara i tehnologa Hrvatske, 61 (9-10), 427-434.

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• Dinnebier, R., Halasz, I., Freyer, D. & Hanson, J. (2011) The Crystal Structures of two Anhydrous Magnesium Hydroxychloride Phases from in situ Synchrotron Powder Diffraction Data. Zeitschrift für anorganische und allgemeine Chemie, 637 (11), 1458-1462 doi:10.1002/zaac.201100139.

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• Ziegler, K., Amsharov, K., Halasz, I. & Jansen, M. (2011) Facile Separation and Crystal Structure Determination of C2-C82(3) Fullerene. Zeitschrift für anorganische und allgemeine Chemie, 637 (11), 1463-1466 doi:10.1002/zaac.201100197.

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• André, V., Hardeman, A., Halasz, I., Stein, R., Jackson, Graham, J., Reid, D., Duer, M., Curfs, C., Duarte, M. & Friščić, T. (2011) Mechanosynthesis of the Metallodrug Bismuth Subsalicylate from Bi2O3 and Structure of Bismuth Salicylate without Auxiliary Organic Ligands. Angewandte Chemie. International edition, 50 (34), 7858-7861 doi:10.1002/anie.201103171.

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• Halasz, I. & Vančik, H. (2011) Surface nucleation in solid-state dimerisation of nitrosobenzenes promoted by sublimation. Crystengcomm, 13, 4307-4310 doi:10.1039/C0CE00870B.

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• Friščić, T., Halasz, I., Strobridge, F., Dinnebier, R., Stein, R., Laszlo, F. & Curfs, C. (2011) A rational approach to screen for hydrated forms of the pharmaceutical derivative magnesium naproxen using liquid-assisted grinding. Crystengcomm, 13 (9), 2125-2129 doi:10.1039/C0CE00894J.

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• Phan, N., Halasz, I., Opahle, I., Alig, E., Fink, L., Bats, J., Cong, P., Lerner, H., Sarkar, B., Wolf, B., Jeschke, H., Lang, M., Valenti, R., Dinnebier, R. & Wagner, M. (2011) Thermally induced crystal-to-crystal transformations accompanied by changes in the magnetic properties of a Cu(II)-p-hydroquinonate polymer. Crystengcomm, 13 (2), 391-395 doi:10.1039/c0ce00367k.

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• Atkinson, M., Halasz, I., Bučar, D., Dinnebier, R., Mariappan, S., Sokolov, A. & MacGillivray, L. (2011) A solid-state trimerisation of a diene diacid affords a bicyclobutyl: reactant structure from X-ray powder data and product separation and structure determination via co-crystallisation. Chemical communications, 47 (1), 236-238 doi:10.1039/C0CC02204G.

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• Halasz, I., Rubčić, M., Užarević, K., Đilović, I. & Meštrović, E. (2011) The cocrystal of 4-oxopimelic acid and 4, 4′-bipyridine: polymorphism and solid-state transformations. New journal of chemistry, 35 (1), 24-27 doi:10.1039/c0nj00569j.

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• Knežević, A., Medančić, T., Milovac, S., Biljan, I., Halasz, I. & Vančik, H. (2011) Photothermal Reactions of Nitrosobenzene and Halonitrosobenzenes in Solid-state. Croatica chemica acta, 84 (1), 21-24 doi:10.5562/cca1714.

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• Halasz, I. & Dinnebier, R. (2010) Molecular Motion by Refinement of TLS Matrices from High Resolution Laboratory Powder Diffraction Data: Implementation in the Program TOPAS and Application to Crystalline Naphthalene. Materials science forum, 651, 65-69 doi:10.4028/www.scientific.net/MSF.651.65.

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• Halasz, I. & Dinnebier, R. (2010) Simulated annealing approach for global minimum verification in modeling of pressure-volume dependence by equations of state obtained by high-pressure diffraction. Materials science forum, 651, 71-77 doi:10.4028/www.scientific.net/MSF.651.71.

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• Halasz, I. (2010) Single-Crystal-to-Single-Crystal Reactivity: Gray, Rather than Black or White. Crystal growth & design, 10, 2817-2823 doi:10.1021/cg100338t.

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• Halasz, I., Dinnebier, R. & Angel, R. (2010) Parametric Rietveld refinement for the evaluation of powder diffraction patterns collected as a function of pressure. Journal of applied crystallography, 43 (3), 504-510 doi:10.1107/S0021889810005856.

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• Friščić, T., Reid, D., Halasz, I., Stein, R., Dinnebier, R. & Duer, M. (2010) Ion- and Liquid-Assisted Grinding: Improved Mechanochemical Synthesis of Metal–Organic Frameworks Reveals Salt Inclusion and Anion Templating. Angewandte Chemie. International edition, 49 (4), 712-715 doi:10.1002/anie.200906583.

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• Locherer, T., Halasz, I., Dinnebier, R. & Jansen Martin (2010) Isothermal compressibility and anisotropic structural response of As2O5 under pressure. Solid State Communications, 150 (3-4), 201-204 doi:10.1016/j.ssc.2009.10.036.

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• Halasz, I. & Dinnebier, R. (2010) Structural and thermal characterization of zolpidem hemitartrate hemihydrate (form E) and its decomposition products by laboratory x-ray powder diffraction. Journal of Pharmaceutical Sciences, 99 (2), 871-878 doi:10.1002/jps.21883.

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• Kandaiah, S., Halasz, I., Dinnebier, R. & Jansen Martin (2009) Electrochemical synthesis and crystal structure of a penta-coordinated silver(II) macrocyclic complex. Inorganica Chimica Acta, 362 (11), 4009-4012 doi:10.1016/j.ica.2009.05.050.

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• Le Bail, A., Cranswick, L., Adil, K., Altomare, A., Avdeev, M., Cerny, R., Giacovazzo, C., Cuocci, C., Halasz, I., Lapidus, S., Louwen, J., Moliterni, A., Palatinus, L., Rizzi, R., Schilder, E., Stephens, P., Stone, K., van Mechelen J. & (2009) Third structure determination by powder diffractometry round robin (SDPDRR-3). Powder Diffraction, 24 (3), 254-262 doi:10.1154/1.3200881.

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• Halasz, I., Biljan, I., Novak, P., Meštrović, E., Plavec, J., Mali, G., Smrečki, V. & Vančik, H. (2009) Cross-dimerization of nitrosobenzenes in solution and in solid state. Journal of molecular structure, 918 (1-3), 19-25 doi:10.1016/j.molstruc.2008.07.035.

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• Alešković, M., Halasz, I., Basarić, N. & Mlinarić-Majerski, K. (2009) Synthesis, structural characterization and anion binding ability of sterically congested adamantane-calix[4]pyrroles and adamantane-calixphyrins. Tetrahedron, 65 (10), 2051-2058 doi:10.1016/j.tet.2009.01.007.

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• Halasz, I., Horvat, M., Biljan, T. & Meštrović, E. (2008) Structural, Spectroscopic and Thermal Characterisation of bis (dibenzoylmethanato)Cd(II) Adducts with Dimethylsulfoxide and Water. Journal of chemical crystallography, 38 (10), 793-800 doi:10.1007/s10870-008-9392-0.

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• Halasz, I., Lukić Kaja & Vančik, H. (2007) Hydrogen phosphate and dihydrogen phosphate salts of 4-aminoazobenzene. Acta Crystallographica - Section C - Crystal Structure Communications, C63 (Part 1), o61-o64 doi::10.1107/S0108270106050979.

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• Judaš, N., Halasz, I. & Bučar, D. (2006) Self-assembly of bis(1, 3-diphenylpropane-1, 3-dionato-kappa2O, O')bis(thiomorpholine-kappaN)cobalt(II). Acta crystallographica. Section E, Structure reports online, 62 (2), m283-m285 doi:10.1107/S1600536806000596.

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• Petrović, V., Halasz, I., Tomić, S. & Matković Čalogović, D. (2006) Methyl 4-O-pivaloyl-beta-D-xylopyranoside. Acta crystallographica. Section E, Structure reports online, 62 (7), o2746-o2748 doi:10.1107/S1600536806021052.

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• Odžak, R., Halasz, I., Tomić, S. & Matković-Čalogović, D. (2006) N-Benzyl-4-(hydroxyiminomethyl)pyridinium bromide. Acta crystallographica. Section E, Structure reports online, 62 (6), o2423-o2424 doi:10.1107/S1600536806018356.

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• Halasz, I., Meštrović, E., Čičak, H., Mihalić, Z. & Vančik, H. (2005) Solid-State Reaction Mechanisms in Monomer-Dimer Interconversions of p- Bromonitrosobenzene. Single-Crystal-to- Single-Crystal Photodissociation and Formation of New Non-van der Waals Close Contact. Journal of Organic Chemistry, 70 (21), 8461-8467.

• Halasz, I., Odžak, R., Tomić, S. & Matković-Čalogović, D. (2005) 2-Bromoethyl 2, 3, 4, 6-tetra-O-acetyl-beta-D-glucopyranoside. Acta crystallographica. Section E, Structure reports online, 61 (8), o2644-o2645 doi:10.1107/S1600536805022555.

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• Vančik, H., Mežnarić-Šimunić, V., Meštrović, E. & Halasz, I. (2004) Nitrosobenzene Dimerizations as a Model System for Studying Solid-State Reaction Mechanisms. Journal of Organic Chemistry, 69 (14), 4829-4834 doi:10.1021/jo049537b.

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• Meštrović, E., Bučar, D., Halasz, I. & Stilinović, V. (2004) The first adduct of bis(1, 3-diphenyl-1, 3-propanedionato)-oxo-vanadium(IV). Acta crystallographica. Section E, Structure reports online, 60 (12), 1920-1922. (https://www.bib.irb.hr/194431).

• Meštrović, E., Halasz, I., Bučar, D. & Žgela, M. (2004) Bis(dimethyl sulfoxide-kappa O)bis(1-phenylbutane-1, 3-dionato-kappa O-2, O ')nickel(II). Acta crystallographica. Section E, Structure reports online, 60 (4), 367-369 doi:10.1107/S1600536804004854.

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