The ion microprobe is located on one of the experimental beamlines (45 degrees) of the RBI accelerator system. It consists of focusing quadrupole magnets, which can operate as a doublet, triplet, or quintuplet depending on the application, and a scattering chamber. The microprobe can utilize ion beams from either of the two tandem accelerators.

In the high-current mode (1 pA to 1 nA), the ion microprobe is used for spectroscopic techniques such as PIXE, RBS, and ERDA:

PIXE (Particle-Induced X-ray Emission) typically uses proton beams of 2–3 MeV focused to approximately 1 micrometer, enabling quantitative elemental analysis of microscopically small samples, as well as mapping of elemental distributions through the detection of characteristic X-rays from all elements heavier than sodium (Z > 11).

RBS (Rutherford Backscattering Spectrometry) is used for depth profiling of elements heavier than the incident beam. For example, when using a helium beam, all elements heavier than lithium can be analyzed. Since the method is sensitive to depth distribution, scanning a focused beam also allows for 3D mapping of elemental distributions.

ERDA (Elastic Recoil Detection Analysis) employs beams of heavier ions to analyze light atoms recoiled from the sample surface. It is particularly useful in the ion microprobe for the detection and quantification of hydrogen.

In the low-current mode (fA range), the ion microprobe is used for techniques based on the interaction of single ions with the target material. In this mode, the beam focus is significantly better than 1 micrometer. The techniques include:

IBIC (Ion Beam Induced Charge) for measuring and imaging charge transport properties in semiconductors.

STIM (Scanning Transmission Ion Microscopy) for mapping thickness (or density) distributions within samples.

TOF MeV SIMS (Time-of-Flight MeV Secondary Ion Mass Spectrometry) for determining the molecular composition of sample surfaces using impacts of heavy ions in the MeV energy range.

General instrument information

Short name
Ion microprobe - nuclear microscopy
Category
kapitalna, odnosno velika (>400.000 EUR)
Analysis type
masena analiza , površinska analiza , spektroskopska analiza , strukturna analiza
Disciplines
Biologija , Fizika , Geofizika , Kemija
Acquisition date
07.04.1994
Financing body
Institut Ruđer Bošković , Ministarstvo znanosti, obrazovanja i mladih Republike Hrvatske , Europska unija , Međunarodna agencija za atomsku energiju
External link

Characteristics

Model
OM-40e
Manufacturer
Oxford Microbeams
Purchase price
500000 EUR
Portability
No
Remote work
No

Location

Address
Bijenička cesta 54
Room
Zgrada VDG akceleratora