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NMR spectra acquisition and interpretation

Category
  • Farmaceutska industrija
  • Medicina
  • Prehrambena industrija
  • Kemijska i petrokemijska industrija

NMR spectra analysis provides valuable information about structure, dynamics and chemical environment of studied molecule.

A request for NMR spectra measurements (PDF form) can be found here and a program for NMR spectra processing can be found here. More advanced NMR processing program can be found at Bruker web pages (free for academic users).

NMR services pricelist can be found here.

Instructions for spectra download from NMR web server can be found here.

NMR spectrometer Bruker Avance 600 is equipped with a 14 T superconducting magnet and three 5 mm diameter probes for liquid state samples: Double resonance ATM broad band probe - PABBO (an observe tunable multinuclear probe, optimized for X-nuclei detection with automatic tuning and matching accessory), Double resonance broad band probe - BBO (an observe tunable multinuclear probe, optimized for X-nuclei detection) and Triple resonance broad band probe - TBI (an inverse tunable multinuclear probe, optimized for 1H detection). Broadband channels with frequency range 24 – 243 MHz can be optimized for nuclei from 107Ag to 31P. All three probes are equipped with a Z-gradient at all frequencies. Measurements can be performed in the temperature range of 223 - 353 K.

NMR spectrometer Bruker Avance 300 is equipped with a 7 T superconducting magnet and two 5 mm diameter probes for liquid state samples:  Double resonance broad band probe - BBO (an observe tunable multinuclear probe, optimized for X-nuclei detection) and Indirect double resonance broad band probe - BBI (an inverse tunable multinuclear probe, optimized for 1H detection). Broadband channels with frequency range 12 – 122 MHz can be optimized for nuclei from 107Ag to 31P. Both probes are equipped with a Z-gradient at all frequencies. Measurements can be performed in the temperature range of 223 - 353 K.

Both instruments are equipped with the autosampler accessory.

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